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Covalent

Failure Analysis Services

Failure analysis services pinpoint why a material, component or device failed. Our scientists combine SEM-EDS, FIB, micro-CT, XPS and more to find the root cause and recommend corrective action.

Root Cause Failure Analysis Lab

Root cause failure analysis for metals, polymers, ceramics, semiconductors and electronic assemblies, from an ISO/IEC 17025-accredited lab in Silicon Valley.

When a part cracks, corrodes, delaminates or stops working, you need to know why. Often you also need evidence that a customer, supplier or court will accept. Our failure analysis lab pairs 75+ analytical instruments with materials scientists who run each investigation from the first inspection to the final report.

What Is Failure Analysis?

Failure analysis is the systematic investigation of why a component, material or product failed. It uses visual inspection, nondestructive testing, microscopy and chemical analysis to identify the failure mode, the mechanism behind it and the root cause, so engineers can correct the problem and keep it from happening again.

An investigation works through three questions in order. First, what happened: the failure mode, such as a fatigue fracture or a short circuit. Second, how it happened: the mechanism, such as cyclic loading concentrated at an undersized fillet radius. Third, why it happened: the design, material, process or service condition that allowed it. Investigations that stop at the failure mode often produce fixes that don't hold.

Research scientist examining samples with a microscope in a lab setting.

When to Order a Failure Analysis

  • A part fails in the field, in qualification testing or on the line, and the cause isn't obvious
  • Warranty returns or customer complaints cluster around one product, lot or supplier
  • Yield drops and your process controls don't explain it
  • You see cracking, corrosion, discoloration, delamination, residue or contamination
  • A supplier dispute, insurance claim or lawsuit needs independent, documented evidence
  • You're qualifying a new material, supplier or process and want to see how it fails before it reaches customers

Types of Failure We Investigate

Failure type

Typical signs

Techniques we use

Fracture and fatigue

Cracks, beach marks, sudden breakage, ductile or brittle fracture surfaces

Stereo microscopy, SEM fractography, metallographic cross-sections, hardness, tensile testing

Corrosion and environmental cracking

Pitting, stress corrosion cracking (SCC), hydrogen embrittlement, galvanic attack

SEM-EDS, XPS, XRD, cross-sections, Auger

Contamination and residues

Haze, films, particles, adhesion loss, outgassing

FTIR, Raman, ToF-SIMS, XPS, GC-MS, SEM-EDS

Coating and adhesion failures

Delamination, blistering, peeling, poor bonding

Cross-sections, SAM, XPS depth profiling, contact angle, FIB-SEM

Polymer and plastic failures

Embrittlement, crazing, warping, discoloration, chemical attack

FTIR, DSC, TGA, DMA, GPC, SEM

Electronic and semiconductor failures

Opens, shorts, leakage, EOS/ESD damage, solder joint cracks, voids

2D X-ray, micro-CT, SAM, FIB-SEM, TEM, cross-sections

Manufacturing and process defects

Porosity, inclusions, voids, weld defects, out-of-spec dimensions

Micro-CT, metallography, optical profilometry, white light interferometry

Thermal damage

Overheating, warpage, CTE mismatch, thermal cycling cracks

TMA, DSC, TGA, cross-sections, SEM

Our Failure Analysis Process

Each investigation moves from nondestructive to destructive methods, so the evidence is documented before anything is cut or altered.

It starts with a scoping call (1). A materials scientist reviews the failure history, the service conditions and the decision you need to make, then sends a test plan and quote. When samples arrive (2), we log and photograph them, and chain-of-custody documentation is available for legal and insurance work.

Nondestructive examination comes next (3). Optical inspection, 2D X-ray, micro-CT and scanning acoustic microscopy locate the defect without changing it. Then targeted destructive analysis (4) uses cross-sectioning, FIB-SEM, fractography and chemical analysis at the failure site. If you can send a passing part, we test it alongside the failed one (5) to separate the cause from normal part-to-part variation.

You get a written report (6) with annotated images, the data, the failure mechanism, the most likely root cause and recommended corrective actions. The scientist who ran the work then walks you through it on a call.

Diagram of the failure analysis process: scoping call, sample intake, nondestructive examination, destructive analysis, comparison with a good part, root cause report
Failure analysis process: (1) scoping call, (2) sample intake with chain of custody, (3) nondestructive examination, (4) targeted destructive analysis, (5) comparison with a good part, (6) root cause report and review call.

Failure Analysis Techniques

Most failure analysis work runs on the 75+ instruments in our Sunnyvale lab, so an investigation can move from X-ray to FIB to surface chemistry without waiting on another facility. When a case needs a technique we don't run in-house, we send that part of the work to a partner lab in our Covalent Connect network. You still work with one Covalent scientist and get one report.

  • Microscopy: SEM, TEM, FIB-SEM, optical and stereo microscopy, white light interferometry
  • Nondestructive inspection: 2D X-ray inspection, micro-CT, scanning acoustic microscopy (SAM)
  • Elemental and surface chemistry: SEM-EDS, XPS, ToF-SIMS, Auger, XRF
  • Molecular and organic analysis: FTIR, Raman, GC-MS
  • Structure and phase: XRD, metallography, mechanical cross-section analysis
  • Thermal and mechanical: DSC, TGA, DMA, TMA, hardness, tensile testing

Industries we support

IndustryTypical failure analysis work
SemiconductorDevice failure analysis at die and package level, delamination, wire bond and bump failures, contamination from process tools
Electronics and PCBASolder joint fatigue, conductive anodic filament, voiding, connector corrosion
Medical devicesImplant and component fractures, polymer degradation, residues relevant to biocompatibility
Aerospace and defenseFatigue and corrosion in structural metals, coating failures, composite delamination
Energy and batteriesElectrode and separator failures, lithium plating, cell swelling, solar module degradation
Industrial and consumer productsCracked housings, failed fasteners and welds, wear, contamination

Failure Analysis Services at Covalent

Our 30,000 ft² lab holds 75+ instruments and more than $25M in instrumentation, so the test plan can follow what the evidence shows. The lab is accredited to ISO/IEC 17025 across 60+ analytical methods, 70% of our staff hold PhDs or advanced degrees, and more than 1,500 companies have sent us work.

You talk directly to the scientist running your samples. Every report includes a plain-language root cause summary, annotated images with the raw data, corrective action recommendations and a review call with that scientist. Chain-of-custody documentation for warranty, insurance, IP or litigation support is available on request. For techniques we don’t run in-house, we can place work through Covalent Connect, our network of trusted partner labs.

Turnaround is typically 5–7 business days, with rush options available at an extra cost.

Frequently Asked Questions

How long does failure analysis take?

Turnaround is typically 5–7 business days, with rush options available at an extra cost. Complex investigations with several techniques may take longer, and we confirm the timeline when we scope the project.

Do you disassemble failed parts and prepare the samples?

Yes. Our team handles disassembly and every stage of sample preparation, including cross-sectioning, polishing and FIB preparation.

What are the warning signs that I need failure analysis right away?

Sudden breakdowns, abnormal electrical or mechanical behavior, or unexplained contamination or defects. Other signs include recurring failures despite process controls, visible cracks or delamination, and significant yield losses.

Can you help with litigation or insurance claims?

Yes. Failure analysis results can support forensic investigations for insurance claims, warranty disputes, intellectual property protection and legal proceedings. You receive a detailed, documented report with high-resolution images and expert interpretation, and chain-of-custody documentation is available.

What information should I include when submitting a failed sample?

Include as much context as possible:

  • Service conditions, such as temperature, load and chemical exposure
  • How long the part was in use
  • The failure symptoms you observed
  • Drawings or specifications, if available
  • Safety documentation, if relevant

What is the difference between a failure mode and a root cause?

The failure mode is what happened, such as a fatigue crack. The root cause is why it happened, such as an undersized fillet radius or a material defect. Fixing only the failure mode often leads to repeat failures.